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Copia del Anexo 1 con los parámetros y ensayos habilitados por la SubSecreataría de Política Ambiental de la provincia de Buenos Aires. Laboratorio habilitado N°: 039, Resolución SPA 026/02 www.opds.gba.gov.ar
MATRICES, PARAMETROS, METODO Y LIMITE DE DETECCION
|
Matriz |
Analito |
Método o Técnica |
Límite de detección |
|
Agua |
Turbidez |
Standard Methods for the Examination of Water and Wastewater 2130 |
0,05 NTU |
|
Agua |
pH |
Standard Methods for the Examination of Water and Wastewater 4500
|
0,02 pH |
|
Agua |
Alcalinidad |
Standard Methods for the Examination of Water and Wastewater 2320 |
0,01 mg/l |
|
Agua |
Dureza |
Standard Methods for the Examination of Water and Wastewater 2340 |
0,01 mg/l |
|
Agua |
Conductividad |
Standard Methods for the Examination of Water and Wastewater 2510 |
0.01 µS/cm |
|
Agua |
Salinidad |
Standard Methods for the Examination of Water and Wastewater 2520 |
0,01 0/00 |
|
Agua |
Sólidos totales |
Standard Methods for the Examination of Water and Wastewater 2540 |
0,001 mg/l |
|
Agua |
Sólidos totales disueltos |
Standard Methods for the Examination of Water and Wastewater 2540 |
0,001 mg/l |
|
Agua |
Sólidos totales en suspensión |
Standard Methods for the Examination of Water and Wastewater 2540 |
0,001 mg/l |
|
Agua |
Sólidos totales volátiles (550°c) |
Standard Methods for the Examination of Water and Wastewater 2540 |
0,001 mg/l |
|
Agua |
Sólidos sedimentables |
Standard Methods for the Examination of Water and Wastewater 2540 |
0,001 mg/l |
|
Agua |
Olor |
Standard Methods for the Examination of Water and Wastewater 2150 |
1 TOD |
|
Agua |
Temperatura |
Standard Methods for the Examination of Water and Wastewater 2550 |
0.01°C |
|
Agua |
OCR (Velocidad de consumo de oxígeno) |
Standard Methods for the Examination of Water and Wastewater 2710 |
0,01 mg O2/gh
|
|
Agua |
Volumen de lodo sedimentable |
Standard Methods for the Examination of Water and Wastewater 2710 |
0,01 ml/l |
|
Agua |
Índice de volumen de lodo |
Standard Methods for the Examination of Water and Wastewater 2710 |
0,01 ml/g |
|
Agua |
Gravedad específica |
Standard Methods for the Examination of Water and Wastewater 2710 |
0,01 (T/4°C) |
|
Agua |
Tiempo de filtrado |
Standard Methods for the Examination of Water and Wastewater 2710 |
1 s/100 ml |
|
Agua |
Manganeso |
US EPA FR 34193 |
0,6 mg/l |
|
Agua |
Arsénico |
US EPA FR 206.4 |
0,04 mg/l |
|
Agua |
Cromo total |
US EPA I -1230-85 |
0,01 mg/l |
|
Agua |
Cobre |
US EPA FR 36166 |
0,02 mg/l |
|
Agua |
Plomo |
US EPA 3500 Pb D |
0,05 mg/l |
|
Agua |
Níquel |
US EPA 3500 Ni D |
0,021 mg/l |
|
Agua |
Zinc |
US EPA FR 36166 |
0,04 mg/l |
|
Agua |
Hierro total |
US EPA FR 43459 |
0,02 mg/l |
|
Agua |
Detergentes SAM |
Standard Methods for the Examination of Water and Wastewater 5540 |
0,05 mg/l |
|
Agua |
Cloro residual |
Standard Methods for the Examination of Water and Wastewater 4500 |
0,01 mg/l |
|
Agua |
Cloro residual |
USEPA 330.5 |
0,01 mg/l |
|
Agua |
Demanda de cloro |
Standard Methods for the Examination of Water and Wastewater 2350 B |
0,1 mg/l |
|
Agua |
Amonio |
Standard Methods for the Examination of Water and Wastewater 4500 US EPA |
0,06 mg/l |
|
Agua |
Nitritos |
Standard Methods for the Examination of Water and Wastewater 4500 USEPA |
0,001 mg/l |
|
Agua |
Nitratos |
Standard Methods for the Examination of Water and Wastewater 4500 |
0,01 mg/l |
|
Agua |
Nitrógeno total |
Standard Methods for the Examination of Water and Wastewater 4500 |
0,2 mg/l |
|
Agua |
N orgánico |
Standard Methods for the Examination of Water and Wastewater 4500 |
0,2 mg/l |
|
Agua |
Clorofila a |
USEPA 445.0 |
0,05 µg/l |
|
Agua |
Feofitina a |
USEPA 445.0 |
0,06 µg/l |
|
Agua |
Oxígeno disuelto |
Standard Methods for the Examination of Water and Wastewater 4500 C- G |
0,1 mg/l |
|
Agua |
Fósforo total |
Standard Methods for the Examination of Water and Wastewater 4500 |
0,2 mg/l |
|
Agua |
Fósforo total |
US EPA 365.2 |
0,2 mg/l |
|
Agua |
Ortofosfatos |
Standard Methods for the Examination of Water and Wastewater 4500 |
0,01 mg/l |
|
Agua |
Ortofosfatos |
US EPA 365.2 |
0,01 mg/l |
|
Agua |
Sulfuro |
Standard Methods for the Examination of Water and Wastewater 4500 |
0,01 mg/l |
|
Agua |
Sulfuro |
US EPA 376.2 |
0,01 mg/l |
|
Agua |
Sulfatos |
Standard Methods for the Examination of Water and Wastewater 4500 |
7 mg/l |
|
Agua |
Sulfatos |
US EPA 375.4 |
7 mg/l |
|
Agua |
Hidrocarburos totales |
Standard Methods for the Examination of Water and Wastewater 5520 |
1 mg/l |
|
Agua |
DBO5 |
Standard Methods for the Examination of Water and Wastewater 5210 |
2 mg/l |
|
Agua |
DQO |
Standard Methods for the Examination of Water and Wastewater 5220 H 8000 US EPA |
5 mg/l |
|
Agua |
Grasas y aceites SSEE |
Standard Methods for the Examination of Water and Wastewater 5520 |
1 mg/l |
|
Agua |
Cloruros |
Standard Methods for the Examination of Water and Wastewater 4500 |
0,5 mg/l |
|
Agua |
Cianuro |
Standard Methods for the Examination of Water and Wastewater 4500 |
0,05 mg/l |
|
Agua |
Fenoles |
Standard Methods for the Examination of Water and Wastewater 5530 – 6420 |
0,003 mg/l |
|
Agua |
Fenoles |
US EPA 420.1 |
0,003 mg/l |
|
Agua |
Plaguicidas organoclorados |
US EPA 8081 a / 8270 C GC-MS |
1µg/l |
|
Agua |
Plaguicidas organofosforados |
US EPA 8141 a GC FID |
1 µg/l |
|
Agua |
Orgánicos semivolátiles |
US EPA 8270 C GC-MS |
10 µg/l |
|
Agua |
Orgánicos volátiles |
Standard Methods for the Examination of Water and Wastewater 6200 |
0,1 µg/l |
|
Agua |
Orgánicos volátiles |
USEPA 8260b |
0,1 µg/l |
|
Agua |
PCB |
US EPA 8270 C GC-MS / 8275 |
10 µg/l |
|
Agua |
Coliformes totales |
Standard Methods for the Examination of Water and Wastewater 9222 – 9223 - 9225 |
1 UFC |
|
Agua |
Coliformes fecales |
Standard Methods for the Examination of Water and Wastewater 9222 – 9223 - 9225 |
1 UFC |
|
Agua |
Ecotoxicidad aguda sobre peces |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
0 |
|
Agua |
Ecotoxicidad con algas dulceacuícolas o marinas |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
0 |
|
Agua |
Ecotoxicidad aguda con CladócerosDaphnia magna |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
0 |
|
Agua |
Ecotoxicidad crónica con CladócerosDaphnia magna |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
0 |
|
Agua |
Ecotoxicidad aguda con Anfípodos:Hyalella curvispina y H. azteca |
US EPA y Di Marzio WD et al. (1999) Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
0 |
|
Agua |
Ecotoxicidad crónica con Anfípodos |
US EPA y Di Marzio WD et al. (1999) Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
0 |
|
Residuos (Semisólidos) |
Sólidos totales, fijados y volátiles |
Standard Methods for the Examination of Water and Wastewater 2540 |
0,001 mg/l |
|
Suelo |
Manganeso |
US EPA FR 34193 |
0,6 mg/l |
|
Suelo |
Arsénico |
US EPA FR 206.4 |
0,04 mg/l |
|
Suelo |
Cromo total |
US EPA I -1230-85 |
0,01 mg/l |
|
Suelo |
Cobre |
US EPA FR 36166 |
0,02 mg/l |
|
Suelo |
Plomo |
US EPA 3500 Pb D |
0,05 mg/l |
|
Suelo |
Níquel |
US EPA 3500 Ni D |
0,021 mg/l |
|
Suelo |
Zinc |
US EPA FR 36166 |
0,04 mg/l |
|
Suelo |
Hierro total |
US EPA FR 43459 |
0,02 mg/l |
|
Suelo |
Sulfuro |
US EPA 376.2 |
0,01 mg/l |
|
Suelo |
Sulfatos |
US EPA 375.4 |
7 mg/l |
|
Suelo |
Fenoles |
US EPA 420.1 |
0,003 mg/l |
|
Suelo |
Plaguicidas organoclorados |
US EPA 8081 a/ 8270 C GC-MS |
660 µg/Kg |
|
Suelo |
Plaguicidas organofosforados |
US EPA 8141 a GC FID |
2 µg/Kg |
|
Suelo |
Orgánicos semivolátiles |
US EPA 8270 C GC-MS |
660 µg/Kg |
|
Suelo |
Orgánicos volátiles |
USEPA 8260b |
0,5 µg/Kg |
|
Suelo |
PCB |
US EPA 8270 C GC-MS / 8275 |
660 µg/Kg |
|
Suelo |
Ecotoxicidad con algas dulceacuícolas o marinas |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
0 |
|
Suelo |
Ecotoxicidad aguda con CladócerosDaphnia magna |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
0 |
|
Suelo |
Ecotoxicidad crónica con CladócerosDaphnia magna |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
0 |
|
Suelo |
Ecotoxicidad aguda con Anfípodos:Hyalella curvispina y H. azteca |
US EPA y Di Marzio WD et al. (1999) Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
0 |
|
Suelo |
Ecotoxicidad crónica con Anfípodos |
US EPA y Di Marzio WD et al. (1999) Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
0 |
|
Suelo |
Ecotoxicidad elongación de raíces y germinación de semillas de lechugaLactuca sativa |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
0 |
|
Suelo |
Ecotoxicidad con lombriz de tierraEisenia foetida |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
0 |
|
Suelos |
Estabilidad de barros |
CEAMSE 1987 |
0,1 mg/l |
|
Suelos |
Líquidos libres |
CEAMSE FR 38 |
0 mg/l |
ANEXO 2
METODOLOGIA PARA LA TOMA DE MUESTRAS
|
Matriz |
Analito |
Metodología |
|
Agua |
Turbidez |
Standard Methods for the Examination of Water and Wastewater 2130 |
|
Agua |
pH |
Standard Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Alcalinidad |
Standard Methods for the Examination of Water and Wastewater 2320 |
|
Agua |
Dureza |
Standard Methods for the Examination of Water and Wastewater 2340 |
|
Agua |
Conductividad |
Standard Methods for the Examination of Water and Wastewater 2510 |
|
Agua |
Salinidad |
Standard Methods for the Examination of Water and Wastewater 2520 |
|
Agua |
Sólidos totales |
Standard Methods for the Examination of Water and Wastewater 2540 |
|
Agua |
Sólidos totales disueltos |
Standard Methods for the Examination of Water and Wastewater 2540 |
|
Agua |
Sólidos totales en suspensión |
Standard Methods for the Examination of Water and Wastewater 2540 |
|
Agua |
Sólidos totales volátiles (550°C) |
Standard Methods for the Examination of Water and Wastewater 2540 |
|
Agua |
Sólidos sedimentables |
Standard Methods for the Examination of Water and Wastewater 2540 |
|
Suelo |
Estabilidad de barros |
CEAMSE 1987 |
|
Suelo |
Líquidos libres |
CEAMSE FR 38 |
|
Residuos (semisólidos) |
Sólidos totales, fijados y volátiles |
Standard Methods for the Examination of Water and Wastewater 2540 |
|
Agua |
Olor |
Standard Methods for the Examination of Water and Wastewater 2150 |
|
Agua |
Temperatura |
Standard Methods for the Examination of Water and Wastewater 2550 |
|
Agua |
OCR (Velocidad de consumo de oxígeno) |
Standard Methods for the Examination of Water and Wastewater 2710 |
|
Agua |
Volumen de lodo sedimentable |
Standard Methods for the Examination of Water and Wastewater 2710 |
|
Agua |
Índice de volumen de lodo |
Standard Methods for the Examination of Water and Wastewater 2710 |
|
Agua |
Gravedad específica |
Standard Methods for the Examination of Water and Wastewater 2710 |
|
Agua |
Tiempo de filtrado |
Standard Methods for the Examination of Water and Wastewater 2710 |
|
Agua |
Manganeso |
US EPA FR 34193 |
|
Suelo |
Manganeso |
US EPA FR 34193 |
|
Agua |
Arsénico |
US EPA 206.4 |
|
Agua |
Cromo total |
US EPA I -1230-85 |
|
Agua |
Cobre |
US EPA FR 36166 |
|
Agua |
Plomo |
US EPA 3500 Pb D |
|
Agua |
Níquel |
US EPA 3500 Ni D |
|
Agua |
Zinc |
US EPA FR 36166 |
|
Agua |
Hierro total |
US EPA FR 43459 |
|
Suelo |
Cromo total |
US EPA I -1230-85 |
|
Suelo |
Cobre |
US EPA FR 36166 |
|
Suelo |
Plomo |
US EPA 3500 Pb D |
|
Suelo |
Níquel |
US EPA 3500 Ni D |
|
Suelo |
Zinc |
US EPA FR 36166 |
|
Suelo |
Hierro total |
US EPA FR 43459 |
|
Agua |
Detergentes SAM |
Standard Methods for the Examination of Water and Wastewater 5540 |
|
Agua |
Cloro residual |
Standard Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Cloro residual |
USEPA 330.5 |
|
Agua |
Demanda de cloro |
Standard Methods for the Examination of Water and Wastewater 2350 B |
|
Agua |
Amonio |
Standard Methods for the Examination of Water and Wastewater 4500 US EPA |
|
Agua |
Nitritos |
Standard Methods for the Examination of Water and Wastewater 4500 US EPA |
|
Agua |
Nitratos |
Standard Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Nitrógeno total |
Standard Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
N Orgánico |
Standard Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Clorofila a |
USEPA 445.0 |
|
Agua |
Feofitina a |
USEPA 445.0 |
|
Agua |
Oxígeno disuelto |
Standard Methods for the Examination of Water and Wastewater 4500 C-G |
|
Agua |
Fósforo total |
Standard Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Ortofosfatos |
Standard Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Sulfuro |
Standard Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Sulfatos |
Standard Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Fósforo total |
US EPA 365.2 |
|
Agua |
Ortofosfatos |
US EPA 365.2 |
|
Agua |
Sulfuro |
US EPA 376.2 |
|
Suelo |
Sulfuro |
US EPA 376.2 |
|
Agua |
Sulfatos |
US EPA 375.4 |
|
Suelo |
Sulfatos |
US EPA 375.4 |
|
Agua |
Hidrocarburos totales |
Standard Methods for the Examination of Water and Wastewater 5520 |
|
Agua |
DBO5 |
Standard Methods for the Examination of Water and Wastewater 5210 |
|
Agua |
DQO |
Standard Methods for the Examination of Water and Wastewater 5220 H 8000 US EPA |
|
Agua |
Grasas y aceites SSEE |
Standard Methods for the Examination of Water and Wastewater 5520 |
|
Agua |
Cloruros |
Standard Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Cianuro |
Standard Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Fenoles |
Standard Methods for the Examination of Water and Wastewater 5530-6420 |
|
Agua |
Fenoles |
US EPA 420.1 |
|
Suelo |
Fenoles |
US EPA 420.1 |
|
Agua |
Plaguicidas organoclorados |
US EPA 8081a/ 8270 C |
|
Agua |
Plaguicidas organofosforados |
US EPA 8141 a |
|
Agua |
Orgánicos semivolátiles |
US EPA 8270 C |
|
Suelo |
Plaguicidas organoclorados |
US EPA 8081a/ 8270 C |
|
Suelo |
Plaguicidas organofosforados |
US EPA 8141 a |
|
Suelo |
Orgánicos semivolátiles |
US EPA 8270 C |
|
Agua |
Orgánicos volátiles |
Standard Methods for the Examination of Water and Wastewater 6200 |
|
Agua |
Orgánicos volátiles |
US EPA 8260b |
|
Suelo |
Orgánicos volátiles |
US EPA 8260b |
|
Agua |
PCB |
US EPA 8270 C / 8275 |
|
Suelo |
PCB |
US EPA 8270 C / 8275 |
|
Suelo |
Liberación de líquidos |
US EPA 9096 |
|
Agua |
Coliformes totales |
Standard Methods for the Examination of Water and Wastewater 9222 – 9223 - 9225 |
|
Agua |
Coliformes fecales |
Standard Methods for the Examination of Water and Wastewater 9222 – 9223 - 9225 |
|
Agua |
Ecotoxicidad con algas dulceacuícolas o marinas |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
|
Agua |
Ecotoxicidad aguda sobre peces |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
|
Suelo |
Ecotoxicidad con algas dulceacuícolas o marinas |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
|
Agua |
Ecotoxicidad aguda con Cladóceros Daphnia magna |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
|
Suelo |
Ecotoxicidad aguda con Cladóceros Daphnia magna |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
|
Agua |
Ecotoxicidad crónica con Cladóceros Daphnia magna |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
|
Suelo |
Ecotoxicidad crónica con Cladóceros Daphnia magna |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
|
Agua |
Ecotoxicidad aguda con Anfípodos: Hyalella curvispina y H. azteca |
US EPA y Di Marzio WD et al.(1999) Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
|
Suelo |
Ecotoxicidad aguda con Anfípodos: Hyalella curvispina y H. azteca |
US EPA y Di Marzio WD et al.(1999) Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
|
Agua
|
Ecotoxicidad crónica con Anfípodos |
US EPA y Di Marzio WD et al.(1999) Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
|
Suelo |
Ecotoxicidad crónica con Anfípodos |
US EPA y Di Marzio WD et al.(1999) Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
|
Suelo |
Ecotoxicidad elongación de raíces y germinación de semillas de lechuga Lactuca sativa |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
|
Suelo |
Ecotoxicidad con lombriz de tierra Eisenia foetida |
Ecological Effects Test Guidelines US EPA 712–C 96—164, 1996 |
 |
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